* 分析測(cè)試新成果

氯化鉀及聚乙二醇對(duì)聚脯氨酸-精氨酸液-液相分離的協(xié)同影響 ························································································································ 項(xiàng)東鑫，鄭 寓，周詩(shī)航，陸 奕，王艷偉 （ 1 ）

交流電弧原子發(fā)射光譜固體粉末樣品制備方法的改進(jìn) ·················· 郭心瑋，郝志紅，姚建貞，白金峰 （ 7 ）

分散固相萃取-超高效液相色譜-串聯(lián)質(zhì)譜法測(cè)定海龍中11 種磺胺類(lèi)抗菌藥物殘留 ································································ 王小喬，李 堅(jiān)，許曉輝，李劍勇，吳福祥，張虹艷，潘秀麗，李 赟 （ 16 ）

濾過(guò)型萃取柱-超高效液相色譜-串聯(lián)質(zhì)譜法同時(shí)測(cè)定水果中11 種農(nóng)藥殘留 ··················································································· 王子劍，趙勁松，郭曉宇，李 倩，鄭天馳，商愛(ài)媛，范 賽 （ 23 ）

藏藥訶子質(zhì)量標(biāo)志物訶黎勒酸的標(biāo)準(zhǔn)化分析研究 ······························································································· 宋志博，陳 濤，王肖波，王岱杰，申 誠(chéng)，王 碩，李洪梅，海 平，李玉林 （140）

敦煌莫高窟壁畫(huà)地仗層可溶鹽遷移過(guò)程模擬研究 ························ 錢(qián) 玲，呂功煊，胡紅巖，陳港泉 （149）

場(chǎng)發(fā)射掃描電子顯微鏡觀測(cè)弱導(dǎo)電金屬有機(jī)框架材料的參數(shù)探究 ······························································································································· 邢宏娜，常 帥，馮 偉，李興華 （160）

一價(jià)/二價(jià)陽(yáng)離子濃度對(duì)蛋白質(zhì)-核酸液液相分離的調(diào)控 ················ 劉柱梁，鄭 寓，周詩(shī)航，王艷偉 （170）

堿性嫩黃O 的光電脫色工藝研究 ····························································································································· 倪賽迪，林秋涵，何碧珊，陳曉達(dá)，郭妙柃，栗鵬輝，林佳麗，陳毅挺 （178）

離子色譜法同時(shí)測(cè)定硫酸氫氯吡格雷中甲酸殘留及硫酸鹽含量 ·································································································································· 馮順卿，卓文珊，王瀟洋，劉洪濤 （185）

直鏈淀粉三(3, 5-二甲基苯基氨基甲酸酯)-聚醚砜手性膜色譜研究 ···················································································································· 普 娜，賴亞琳，高順秋，蔣雪菲，袁黎明 （280）

蒙藥十八味歐曲丸中游離汞的含量測(cè)定 ···································· 馬 蕊，丁玉竹，哈 偉，師彥平 （286）

基于鎳鉬硫化物納米花修飾碳納米管的腦利鈉肽電化學(xué)免疫傳感器的構(gòu)建 ··················································································································· 李 燕，朱長(zhǎng)慧，代玉雪，李志英 （292）

頂空氣相色譜-電子捕獲檢測(cè)器法測(cè)定明膠空心膠囊中2-氯乙醇?xì)埩袅?························································································································ 程 磊，郭文旭，王丹丹，陳 超 （299）

超聲萃取-氣相色譜法測(cè)定擬南芥種子中脂肪酸含量 ···················· 宜原原，羅 云，阮梅林，雷 敏 （339）

材料孔隙率測(cè)試方法的研究 ···················· 陳佩麗，宋 達(dá)，鄧金林，范明旸，陳曉麗，付 娟，蘇秋成 （347）

基于X射線光電子能譜的絕緣柵雙極型晶體管失效分析 ································································································································ 章小余，趙志娟，劉 芬，徐 鵬，屈寶龍 （352）

星狀風(fēng)毛菊藥材分析及質(zhì)量標(biāo)準(zhǔn)研究 ·············································································································· 馬家麟，王 碩，陳 濤，宋 霞，喬亞玲，杲秀珍，申 誠(chéng)，海 平，李玉林 （357）

* 大型儀器功能開(kāi)發(fā)

正負(fù)壓一體式無(wú)空氣X射線光電子能譜原位轉(zhuǎn)移倉(cāng)的開(kāi)發(fā)及研制 ······························································································································· 章小余，趙志娟，袁 震，劉 芬 （ 30 ）

模擬空間原子氧輻照下X射線光電子能譜儀的原位表征功能開(kāi)發(fā) ······························································································································· 劉 建，剡 珍，郝俊英，劉維民 （ 37 ）

高低溫環(huán)境下紅外光譜原位表征系統(tǒng)的研制 ···················· 郭 艷，許傳芝，王 嘉，張樂(lè)芬，牛建中 （ 43 ）

一種液體吸附原位紅外表征系統(tǒng) ··································· 郭 艷，許傳芝，王 嘉，張樂(lè)芬，牛建中 （216）

近紅外輕質(zhì)油品快速檢測(cè)系統(tǒng)的研制和應(yīng)用 ······························································ 陳國(guó)鈺 （221）

X-射線單晶衍射儀XtaLAB Pro 的低溫系統(tǒng)改造 ···································· 馬 宣，孫愛(ài)君，張 云 （227）

自補(bǔ)償型雙擺式干涉儀的設(shè)計(jì) ················································ 石 磊，孫長(zhǎng)庫(kù)，夏恒新，李巖松 （304）

* 大型儀器科學(xué)管理

高校儀器共享平臺(tái)檔案信息化管理模式探索 ······························ 李艷偉，盛弘強(qiáng)，方三華，劉 麗 （ 49 ）

我國(guó)民營(yíng)第三方檢測(cè)服務(wù)現(xiàn)狀及趨勢(shì) ···························································· 張志強(qiáng)，王麗紅 （334）

校級(jí)分析測(cè)試中心大型儀器設(shè)備共享平臺(tái)建設(shè)探討——以西南交通大學(xué)分析測(cè)試中心為例 ·················································································································· 衛(wèi)飛飛，方維臻 （429）

“四個(gè)最大”和“四個(gè)最小”的大型精密貴重儀器全生命周期管理體系的構(gòu)建 ················· 薛青松 （438）

* 浙江省大型科研儀器開(kāi)放共享平臺(tái)—質(zhì)譜專欄

牛奶中全氟烷基酸的簡(jiǎn)便萃取與定量研究 ············································ 李城華，汪 嫣，蔣可志 （ 54 ）

基于串聯(lián)質(zhì)量標(biāo)簽定量質(zhì)譜法的膠質(zhì)瘤外泌體蛋白組差異分析 ··························· 裴順琪，譚 舟 （ 63 ）

基于氣相色譜三重四極桿質(zhì)譜法分析5 種苯系物在貽貝體內(nèi)的分布、蓄積和消除規(guī)律 ················································································ 晁鐸源，宋立玲，王紅光，丁 顒，邵宏宏，周秀錦 （ 68 ）

Cocktail 探針?biāo)幬锓ㄔu(píng)價(jià)玄參對(duì)大鼠細(xì)胞色素P450 酶的影響 ····································································································· 魏艷麗，應(yīng)曉倩，談文狀，吳美玲，江悅娟，丁明星，杜洪建 （ 76 ）

質(zhì)譜在金屬有機(jī)框架材料結(jié)構(gòu)與應(yīng)用表征上的研究進(jìn)展 ·························· 陳銀娟，丁傳凡，盧星宇 （ 83 ）

質(zhì)譜分析在變壓器所用礦物絕緣油成分分析中的應(yīng)用 ·················································· 劉佳蓉 （ 93 ）

離子色譜法測(cè)定廢水中的六氟磷酸根 ······································································· 趙 薇 （101）

* 分析測(cè)試經(jīng)驗(yàn)介紹

加速溶劑萃取-QuEChERS-氣相色譜質(zhì)譜聯(lián)用法測(cè)定土壤中增塑劑 ······················· 唐會(huì)智，宋冬梅 （105）

原位變溫X射線衍射測(cè)試技術(shù)及其影響因素 ········· 毛 晶，郭倩穎，馬利利，龍麗霞，韓雅靜，馬曉暉 （111）

會(huì)理地區(qū)種植基地果蔬中農(nóng)藥殘留現(xiàn)狀與分析 ··································· 陳明華，曾 艷，歐陽(yáng)衛(wèi)民 （117）

綜合物性測(cè)量系統(tǒng)振動(dòng)樣品磁強(qiáng)計(jì)測(cè)量定中心問(wèn)題的探究 ······················· 馬 麟，王 朔，王 維 （191）

利用Visual Basic 自動(dòng)編制分析測(cè)試報(bào)告 ·································· 傅澤華，王如海，孫玉芳，唐昊冶 （197）

激光共聚焦顯微鏡測(cè)量表面粗糙度的探究 ············································ 廖奕鷗，馮 輝，張重遠(yuǎn) （203）

不同參數(shù)優(yōu)化對(duì)ZSM-5 分子篩的掃描電子顯微鏡圖像影響 ································ 王馨楠，高占明 （209）

木質(zhì)纖維素材料前處理的方法 ····································································· 王小曼，王 聞 （309）

無(wú)窗X射線能譜在熒光樣品與金屬鋰成分分析中的優(yōu)勢(shì)與經(jīng)驗(yàn)摸索 ·················································································· 萬(wàn) 鵬，蔡 蕊，李 勇，孟祥玉，周雨萌，高曉霞，徐 強(qiáng)，閆 肅 （313）

測(cè)量系統(tǒng)分析在大米鎘、鉛元素檢測(cè)中的應(yīng)用研究 ······················ 韋 冰，蔣菊媛，覃均生，張倩勉 （321）

電感耦合等離子體質(zhì)譜法測(cè)定鎂合金中的痕量元素 ····················································· 黃丹宇 （328）

QuEChERS-高效液相色譜/三重四極桿質(zhì)譜聯(lián)用法測(cè)定化妝品中防曬劑的檢測(cè)方法 ···················································································· 潘秀麗，邵長(zhǎng)春，李 赟，許曉輝，王小喬，張虹艷 （384）

熟地黃的炮制及有效成分和微量元素的檢測(cè)研究 ···················································································································· 陳勝?gòu)?qiáng)，楊克培，康文利，周永昌，陶思曼，關(guān)伊辰，蒲秀瑛 （392）

粉末樣品制備方法對(duì)掃描電子顯微鏡成像質(zhì)量的影響 ·················································· 王馨楠 （400）

微波灰化-電感耦合等離子體發(fā)射光譜法測(cè)定嬰幼兒乳粉中的鈣和磷 ······································································································ 陳麗梅，張 慧，白國(guó)濤，馬彩霞，姚思雨，王 婧 （407）

苯系物相對(duì)質(zhì)量校正因子的測(cè)定與比較分析 ··················································· 李紫騰，李 盼 （414）

高效液相色譜法測(cè)定化妝品中類(lèi)視黃醇含量 ······························ 羊潔芳，樓美娟，盧 力，姜士磊 （421）

* 綜 述

基于金屬有機(jī)框架材料的酶固定化策略及藥物篩選研究進(jìn)展 ··························································································· 常香蕾，張 瑛，Stanislas Nsanzamahoro，王鋮博，王偉峰，楊軍麗 （125）

行波離子遷移譜技術(shù)及應(yīng)用研究進(jìn)展 ························································································································· 潘慢慢，李 杭，徐一仟，楊其穆，蔣丹丹，王衛(wèi)國(guó)，陳 創(chuàng)，李海洋 （231）

原位高分辨微區(qū)元素分布特征檢測(cè)技術(shù)的應(yīng)用進(jìn)展 ····················· 林梵宇，尹希杰，劉建鑫，孫延鑫 （245）

便攜式毒品傳感器的應(yīng)用與研究進(jìn)展 ······································································· 楊 春 （261）

紫外光化學(xué)蒸氣發(fā)生技術(shù)綜述 ··························· 郭 煒，劉美彤，張衛(wèi)宏，葛迎吉，康 寧，劉子杰 （272）

地下建筑內(nèi)氡分布與去除技術(shù)研究進(jìn)展 ··············································· 呂功煊，甄文龍，寧曉峰 （364）

* 大型儀器維護(hù)與維修

EA3000-CHNS 測(cè)試的影響因素與解決方案 ······························· 郭 毅，張瀅瀅，張歆寧，倪旭峰 （378）