*大型儀器維護與維修

RFDA-HTVP-1750C 高溫動態(tài)彈性模量與阻尼分析儀的維護與常見問題探討 ······························· ··························································································余建新，焦 陽，王曉鵬 （ 1 ）

HydraⅡ C 自動測汞儀兩例故障分析及排除 ··· 王 東，孫春曉，王 偉，馬 玲，呂新明，徐新忠 （2 2 8）

原子吸收分光光度計石墨爐原子化法故障排除及原因分析 ······················································ ······················································余政軍，尹小紅，李海林，楊 柳，畢晶秀，傅志強 （3 0 8）

Isoprime 100穩(wěn)定性同位素比質譜儀故障分析及排除 ··························· 谷淑波，徐 毅，金 敏 （4 7 3）

EVO MA 15鎢燈絲掃描電子顯微鏡的日常維護 ············································· 陳新芳，周靜韻 （4 8 0）

*綜述

氮川三乙酸的樣品前處理和檢測方法研究進展 ··································· 程嘉雯，馬繼平，田 永 （ 8 ）

離子色譜法在中藥化學成分分析中的應用進展 ····································································· ····················································· 頡東妹，魏晗婷，王寧麗，劉建飛，郭 玫，邸多隆 （1 7 9）

調節(jié)三高類中成藥和保健食品中非法添加化學藥物及其檢測研究進展 ····· 李文斌，張 萍，徐 瑩 （1 8 8）

光譜法水質監(jiān)測儀器和方法國內專利狀況分析 ····································································· ····················································· 常璽鳳，虞功亮，韓璐璐，王 濤，時安琪，喬之怡 （3 1 2）

基于CiteSpace的實驗隊伍研究熱點和趨勢 ··················································· 岳 琦，王 晉 （3 2 0）

生物質炭的制備及其在吸附中的應用 ··································· 丁娜娜，梁錦華，烏 蘭，張海霞 （3 6 3）

基質輔助激光解析電離飛行時間質譜分析合成聚合物樣品制備的研究進展 ······················· 代莉莉 （3 7 5）

毛細管電泳在生物大分子分析中的應用研究進展 ···················· 彭 樂，程佳偉，李淑楠，李文龍 （3 8 4）

*浙江省大型科研儀器開放共享平臺－國產科研儀器研發(fā)與應用專欄

智能數(shù)字聚合酶鏈式反應系統(tǒng)的開發(fā)與應用驗證 ···················· 尚君鵬，賀曉偉，方秋雨，牟 穎 （ 18 ）

數(shù)智物聯(lián)巖石力學背包實驗室的自主創(chuàng)新 ····························· 伍 劼，伍法權，喬 磊，張 芳 （ 24 ）

二維核磁共振技術解析鹽酸帕羅西汀 ······································································· 毛偵軍 （ 31 ）

基于波數(shù)校準下傅里葉紅外氣體分析儀模型傳遞的研究 ························································· ············································ 查麗霞，周新奇，陳 磊，尚慶賀，王 兵，李康康，周志明 （ 37 ）

高效液相色譜法快速測定參芪降糖膠囊中人參皂苷的含量 ································ 林靈超，黃 燕 （ 45 ）

頂空-氣相色譜法測定水中三氯甲烷和四氯化碳方法的改進 ··················· 王瓊瓊，黃翌磊，李俊珂 （ 51 ）

浙江省國產科研儀器發(fā)展現(xiàn)狀分析及對策 ····························· 陳 盼，陳 寧，亓云濤，趙志娟 （ 57 ）

加快推進國產科研儀器“進口替代”的思考 ·············· 袁 勇，付國春，戴靈豪，謝曉笑，張燕勤 （ 62 ）

*分析測試新成果

固相萃取-氣相色譜-質譜法測定3種中藥材中 18種多環(huán)芳烴 ················ 李文斌，池艷艷，程 菲 （ 68 ）

固體進樣-石墨爐原子吸收法測定農產品中重金屬元素含量 ······· 莫 輝，游曉瑩，潘小平，池巧東 （ 80 ）

長慶油田石油磺酸鹽中活性組分識別 ················································································· ········································· 徐飛艷，王永宏，張 英，馮春艷，李文宏，王 帥，郭 勇 （ 88 ）

響應面優(yōu)化微波輔助Fenton法降解活性艷藍KN-R ······························································· ········································· 林曉森，薛祥航，董慧敏，方淑兵，丁美琪，賴紫宣，陳毅挺 （1 4 4）

高溫比熱容測試常見問題及誤差分析 ······················· 焦 陽，劉春鳳，王曉鵬，孫昭媛，余建新 （1 5 3）

Co3O4/CeO2復合電極材料的制備與超級電容器電化學性能研究 ························· 唐明華，王 穎 （4 0 0）

超高效合相色譜法測定纈沙坦原料藥中R-纈沙坦 ·································································· ····················································· 丁建營，劉發(fā)貴，王 花，劉思光，李鐵健，張貴民 （4 0 5）

高效液相色譜法測定磷酸三甲苯酯中游離甲酚的含量 ·························· 王世平，牛靜靜，杜亞珍 （4 1 1）

金銀花綠原酸提取方法研究 ··································· 李 輝，逯桃桃，陳 佳，趙 亮，邱洪燈 （4 1 6）

*分析測試經驗介紹

QuEChERS-超高效液相色譜串聯(lián)質譜法快速測定嬰幼兒奶粉中5種黃曲霉毒素含量 ····················· ····························· 王小喬，許曉輝，張虹艷，馮 翀，吳福祥，潘秀麗，李 赟，李晨曦 （ 96 ）

高效液相色譜法測定鎳鍍液中的糖精鈉和苯亞磺酸鈉 ···························································· ········································· 王 焱，董玉坤，李瑞基，馮建華，郭 勇，盧曉鋒，李亦婧 （1 0 3）

微波消解-電感耦合等離子體質譜法測定血液中 30 種微量元素 ················································· ············································································· 火 婷，毛寶宏，李亞麗，任 偉 （1 9 8）

氣相色譜法測定煙草浸膏中的煙堿 ·············· 肯生葉，段 勤，蘇丹丹，楊 屹，田飛宇，楊雪燕 （2 0 5）

玻璃類注射劑用藥包材內表面耐受性測試研究 ··············································· 聶 蕾，范 旭 （2 1 0）

上游水庫水體中氨氮、亞硝酸鹽氮、硝酸鹽氮、總氮的測定和關系探究 ···························· 趙文斌 （2 2 2）

氣相色譜柱對多溴聯(lián)苯醚分析的影響 ··································· 張 煒，馮 灝，張 冰，楊永壇 （3 2 7）

基于CIRAS-3光合儀的CO2響應曲線測定 ··············· 饒心雨，楊翠珍，李永平，李自文，宋志姣 （3 3 4）

基于氣相色譜-質譜和網絡藥理學探討紫斑罌粟殼揮發(fā)油鎮(zhèn)咳祛痰平喘的作用機制 ······················· ····· 宋小蘭，王麗萍，趙寧娟，李建慧，楊 璐，王 諾，康文利，王小忠，張 偉，武全香 （3 4 3）

高效液相色譜-二極管陣列檢測器法測定復方丹參片中12種成分及摻偽鑒別 ········ 范可青，凌 霞 （3 5 3）

電感耦合等離子體發(fā)射光譜法測定鋁合金中的多種金屬元素 ········································· 孫永放 （3 5 8）

微波消解-電感耦合等離子體原子發(fā)射光譜法測定鉬鐵合金中的鉬含量 ······································ ····················································· 趙炳建，趙浩年，趙 越，史 琦，李小林，袁 輝 （4 2 2）

電感耦合等離子體質譜法測定地龍藥材中鉛、砷、汞、鎘、銅元素的殘留量 ·································· ································································· 馬 彧，李正剛，曲涵婷，趙 艷，王路宏 （4 2 7）

冷凍掃描電子顯微鏡冷凍斷裂法在生物樣品觀察中的應用 ······················································ ····················································· 黃克讓，王 珍，陳 蕾，崔鳳展，彭潔瑩，張 敏 （4 3 3）

超高效液相色譜-串聯(lián)質譜法同時測定化妝品中50種非法添加藥物 ···················· 廖文榕，黃健浩 （4 3 9）

電感耦合等離子體發(fā)射光譜法測定三氯化釕溶液中雜質元素含量 ············································· ································································· 張玉德，劉榮正，羅 雄，崇 彪，白文剛 （4 5 1）

偏光顯微鏡與X射線衍射儀聯(lián)用技術測定化妝品中石棉含量 ···· 張 雷，蘇粉良，王海瑞，胡積東 （4 5 7）

粉末X射線衍射法測定消咳寧片中碳酸鈣含量 ······················ 張建平，孫倩男，周雪梅，王 棟 （4 6 3）

樹脂包埋在透射電子顯微鏡測試中的應用 ········································· 王小曼，梁 正，盧 思 （4 6 9）

*大型儀器科學管理

中國科學院檢驗檢測機構資質認定概況 ························································ 申孟芝，張紅松 （1 0 8）

質譜平臺的運行管理和開放共享 ············································································· 盧巧梅 （1 5 9）

大型科學儀器專業(yè)技術培訓促進使用效益提升的思考 ···························································· ········································· 張麗娜，楊 娟，吳愛華，包郁明，巫祥云，孫瑩璐，韓玉剛 （1 6 3）

*浙江省大型科研儀器開放共享平臺–電子顯微鏡專欄

<113>c晶帶軸下Ba(B'1/3B″2/3)O3鈣鈦礦B位 1∶2 有序結構的透射電鏡表征 ······························ ············································································· 馬翩翩，劉觀福，喬 茵，徐人豪 （1 1 3）

釤鈷合金等溫時效過程中胞狀組織結構的透射電鏡表征 ························································· ································································· 吳海辰，劉 壯，王新明，陳國新，盧煥明 （1 1 8）

導電環(huán)氧樹脂消除掃描電子顯微鏡圖像荷電問題的原理與實踐 ················································ ·············································································· 彭 宇，張之恒，安 婷，錢匡亮（1 2 5）

掃描電子顯微鏡在緩釋微球制劑表征中的應用進展 ················· 陳 超，樊海麗，蔡志威，張傳杰 （1 3 2）

pH調控水熱法合成BiVO4及其可見光催化降解甲基橙 ··········· 秦玉嬌，蔣琦銳，張智芝，王林霞 （1 3 9）

純鋅中變形孿晶界精細結構的透射電子顯微鏡表征 ······························································· ····················································· 吳海辰，陳國新，于海濤，沈圣成，梁 芮，盧煥明 （2 4 7）

掃描電子顯微鏡和能譜分析高性能熱塑性板材 ····································································· ········································· 鄭 娜，徐 麗，沈素丹，賀 靜，房爾園，浦 群，介素云 （2 5 4）

掃描電子顯微鏡-能譜聯(lián)用在鑒別藥包材上的應用 ······························· 蔡志威，梁鍵謀，陳 超 （2 6 0）

新氫壓縮機活塞桿斷裂原因分析 ····· 姚懿容，蔣蓉蓉，段北晨，管建敏，熊發(fā)浩，李 明，盧煥明 （2 6 7）

掃描電子顯微鏡在鵪鶉蛋殼表征中的應用 ····················································· 鄭 希，戎念杭 （2 7 3）

掃描透射電子顯微鏡技術及其在中藥研究中的應用 ····················································· 王月霞 （2 8 0）

掃描電子顯微鏡運行和管理的實踐與探索 ····························· 何益超，盛國棟，陳朝貴，王林霞 （2 8 9）

*浙江省大型科研儀器開放共享平臺-大型科研儀器開放共享管理研究專欄

高校大型科研儀器開放共享運行機制探究 ········································· 亓文濤，陳 盼，高 然 （1 6 7）

高校和科研院所分析測試中心質量管理體系重要性和建設舉措探究 ·········································· ································································· 張 麗，李子厚，陳 波，賈亞茹，戚淑燕 （1 7 3）

*研究報告

聚（異丙基甲基丙烯酰胺）@聚（N-異丙基丙烯酰胺）中空微凝膠合成過程的形態(tài)學表征 ··················· ············································································· 郭宏博，白 露，胡西學，孫 迪 （2 3 3）

脫氧核糖核酸變性和損傷的原子力顯微鏡液相觀察 ······························································· ··········································駱蕓爾，高 珊，伊 藝，陸 奕，鄭 寓，王艷偉，潘海鷗 （2 4 1）

*分析測試新方法

電感耦合等離子體質譜法測定新型抗菌不銹鋼在生理鹽水和磷酸鹽緩沖液中的鎵溶出量 ··············· ························································································· 于英杰，李 輝，張重遠 （2 9 3）

無衍生化-氣相色譜法測定藥用膠塞提取液中硬脂酸和棕櫚酸 ·················································· ································································· 余秋玲，馬 艷，謝 威，楊 倩，龍 梅 （2 9 9）

離子色譜法快速測定氯化鉀中微量溴離子和硫酸根離子 ··································· 金 珍，閆春輝 （3 0 4）

*大型儀器功能開發(fā)

物理吸附系統(tǒng)的改造及其測試 ···················· 陳佩麗，王樹加，陳凱悅，陳曉麗，付 娟，蘇秋成 （3 9 2）