*大型儀器維護與維修

RFDA-HTVP-1750C 高溫動態(tài)彈性模量與阻尼分析儀的維護與常見問題探討 ······························· ··························································································余建新，焦 陽，王曉鵬 （ 1 ）

HydraⅡ C 自動測汞儀兩例故障分析及排除 ··· 王 東，孫春曉，王 偉，馬 玲，呂新明，徐新忠 （2 2 8）

原子吸收分光光度計石墨爐原子化法故障排除及原因分析 ······················································ ······················································余政軍，尹小紅，李海林，楊 柳，畢晶秀，傅志強 （3 0 8）

Isoprime 100穩(wěn)定性同位素比質(zhì)譜儀故障分析及排除 ··························· 谷淑波，徐 毅，金 敏 （4 7 3）

EVO MA 15鎢燈絲掃描電子顯微鏡的日常維護 ············································· 陳新芳，周靜韻 （4 8 0）

*綜述

氮川三乙酸的樣品前處理和檢測方法研究進展 ··································· 程嘉雯，馬繼平，田 永 （ 8 ）

離子色譜法在中藥化學成分分析中的應用進展 ····································································· ····················································· 頡東妹，魏晗婷，王寧麗，劉建飛，郭 玫，邸多隆 （1 7 9）

調(diào)節(jié)三高類中成藥和保健食品中非法添加化學藥物及其檢測研究進展 ····· 李文斌，張 萍，徐 瑩 （1 8 8）

光譜法水質(zhì)監(jiān)測儀器和方法國內(nèi)專利狀況分析 ····································································· ····················································· 常璽鳳，虞功亮，韓璐璐，王 濤，時安琪，喬之怡 （3 1 2）

基于CiteSpace的實驗隊伍研究熱點和趨勢 ··················································· 岳 琦，王 晉 （3 2 0）

生物質(zhì)炭的制備及其在吸附中的應用 ··································· 丁娜娜，梁錦華，烏 蘭，張海霞 （3 6 3）

基質(zhì)輔助激光解析電離飛行時間質(zhì)譜分析合成聚合物樣品制備的研究進展 ······················· 代莉莉 （3 7 5）

毛細管電泳在生物大分子分析中的應用研究進展 ···················· 彭 樂，程佳偉，李淑楠，李文龍 （3 8 4）

*浙江省大型科研儀器開放共享平臺－國產(chǎn)科研儀器研發(fā)與應用專欄

智能數(shù)字聚合酶鏈式反應系統(tǒng)的開發(fā)與應用驗證 ···················· 尚君鵬，賀曉偉，方秋雨，牟 穎 （ 18 ）

數(shù)智物聯(lián)巖石力學背包實驗室的自主創(chuàng)新 ····························· 伍 劼，伍法權(quán)，喬 磊，張 芳 （ 24 ）

二維核磁共振技術解析鹽酸帕羅西汀 ······································································· 毛偵軍 （ 31 ）

基于波數(shù)校準下傅里葉紅外氣體分析儀模型傳遞的研究 ························································· ············································ 查麗霞，周新奇，陳 磊，尚慶賀，王 兵，李康康，周志明 （ 37 ）

高效液相色譜法快速測定參芪降糖膠囊中人參皂苷的含量 ································ 林靈超，黃 燕 （ 45 ）

頂空-氣相色譜法測定水中三氯甲烷和四氯化碳方法的改進 ··················· 王瓊瓊，黃翌磊，李俊珂 （ 51 ）

浙江省國產(chǎn)科研儀器發(fā)展現(xiàn)狀分析及對策 ····························· 陳 盼，陳 寧，亓云濤，趙志娟 （ 57 ）

加快推進國產(chǎn)科研儀器“進口替代”的思考 ·············· 袁 勇，付國春，戴靈豪，謝曉笑，張燕勤 （ 62 ）

*分析測試新成果

固相萃取-氣相色譜-質(zhì)譜法測定3種中藥材中 18種多環(huán)芳烴 ················ 李文斌，池艷艷，程 菲 （ 68 ）

固體進樣-石墨爐原子吸收法測定農(nóng)產(chǎn)品中重金屬元素含量 ······· 莫 輝，游曉瑩，潘小平，池巧東 （ 80 ）

長慶油田石油磺酸鹽中活性組分識別 ················································································· ········································· 徐飛艷，王永宏，張 英，馮春艷，李文宏，王 帥，郭 勇 （ 88 ）

響應面優(yōu)化微波輔助Fenton法降解活性艷藍KN-R ······························································· ········································· 林曉森，薛祥航，董慧敏，方淑兵，丁美琪，賴紫宣，陳毅挺 （1 4 4）

高溫比熱容測試常見問題及誤差分析 ······················· 焦 陽，劉春鳳，王曉鵬，孫昭媛，余建新 （1 5 3）

Co3O4/CeO2復合電極材料的制備與超級電容器電化學性能研究 ························· 唐明華，王 穎 （4 0 0）

超高效合相色譜法測定纈沙坦原料藥中R-纈沙坦 ·································································· ····················································· 丁建營，劉發(fā)貴，王 花，劉思光，李鐵健，張貴民 （4 0 5）

高效液相色譜法測定磷酸三甲苯酯中游離甲酚的含量 ·························· 王世平，牛靜靜，杜亞珍 （4 1 1）

金銀花綠原酸提取方法研究 ··································· 李 輝，逯桃桃，陳 佳，趙 亮，邱洪燈 （4 1 6）

*分析測試經(jīng)驗介紹

QuEChERS-超高效液相色譜串聯(lián)質(zhì)譜法快速測定嬰幼兒奶粉中5種黃曲霉毒素含量 ····················· ····························· 王小喬，許曉輝，張虹艷，馮 翀，吳福祥，潘秀麗，李 赟，李晨曦 （ 96 ）

高效液相色譜法測定鎳鍍液中的糖精鈉和苯亞磺酸鈉 ···························································· ········································· 王 焱，董玉坤，李瑞基，馮建華，郭 勇，盧曉鋒，李亦婧 （1 0 3）

微波消解-電感耦合等離子體質(zhì)譜法測定血液中 30 種微量元素 ················································· ············································································· 火 婷，毛寶宏，李亞麗，任 偉 （1 9 8）

氣相色譜法測定煙草浸膏中的煙堿 ·············· 肯生葉，段 勤，蘇丹丹，楊 屹，田飛宇，楊雪燕 （2 0 5）

玻璃類注射劑用藥包材內(nèi)表面耐受性測試研究 ··············································· 聶 蕾，范 旭 （2 1 0）

上游水庫水體中氨氮、亞硝酸鹽氮、硝酸鹽氮、總氮的測定和關系探究 ···························· 趙文斌 （2 2 2）

氣相色譜柱對多溴聯(lián)苯醚分析的影響 ··································· 張 煒，馮 灝，張 冰，楊永壇 （3 2 7）

基于CIRAS-3光合儀的CO2響應曲線測定 ··············· 饒心雨，楊翠珍，李永平，李自文，宋志姣 （3 3 4）

基于氣相色譜-質(zhì)譜和網(wǎng)絡藥理學探討紫斑罌粟殼揮發(fā)油鎮(zhèn)咳祛痰平喘的作用機制 ······················· ····· 宋小蘭，王麗萍，趙寧娟，李建慧，楊 璐，王 諾，康文利，王小忠，張 偉，武全香 （3 4 3）

高效液相色譜-二極管陣列檢測器法測定復方丹參片中12種成分及摻偽鑒別 ········ 范可青，凌 霞 （3 5 3）

電感耦合等離子體發(fā)射光譜法測定鋁合金中的多種金屬元素 ········································· 孫永放 （3 5 8）

微波消解-電感耦合等離子體原子發(fā)射光譜法測定鉬鐵合金中的鉬含量 ······································ ····················································· 趙炳建，趙浩年，趙 越，史 琦，李小林，袁 輝 （4 2 2）

電感耦合等離子體質(zhì)譜法測定地龍藥材中鉛、砷、汞、鎘、銅元素的殘留量 ·································· ································································· 馬 彧，李正剛，曲涵婷，趙 艷，王路宏 （4 2 7）

冷凍掃描電子顯微鏡冷凍斷裂法在生物樣品觀察中的應用 ······················································ ····················································· 黃克讓，王 珍，陳 蕾，崔鳳展，彭潔瑩，張 敏 （4 3 3）

超高效液相色譜-串聯(lián)質(zhì)譜法同時測定化妝品中50種非法添加藥物 ···················· 廖文榕，黃健浩 （4 3 9）

電感耦合等離子體發(fā)射光譜法測定三氯化釕溶液中雜質(zhì)元素含量 ············································· ································································· 張玉德，劉榮正，羅 雄，崇 彪，白文剛 （4 5 1）

偏光顯微鏡與X射線衍射儀聯(lián)用技術測定化妝品中石棉含量 ···· 張 雷，蘇粉良，王海瑞，胡積東 （4 5 7）

粉末X射線衍射法測定消咳寧片中碳酸鈣含量 ······················ 張建平，孫倩男，周雪梅，王 棟 （4 6 3）

樹脂包埋在透射電子顯微鏡測試中的應用 ········································· 王小曼，梁 正，盧 思 （4 6 9）

*大型儀器科學管理

中國科學院檢驗檢測機構(gòu)資質(zhì)認定概況 ························································ 申孟芝，張紅松 （1 0 8）

質(zhì)譜平臺的運行管理和開放共享 ············································································· 盧巧梅 （1 5 9）

大型科學儀器專業(yè)技術培訓促進使用效益提升的思考 ···························································· ········································· 張麗娜，楊 娟，吳愛華，包郁明，巫祥云，孫瑩璐，韓玉剛 （1 6 3）

*浙江省大型科研儀器開放共享平臺–電子顯微鏡專欄

<113>c晶帶軸下Ba(B'1/3B″2/3)O3鈣鈦礦B位 1∶2 有序結(jié)構(gòu)的透射電鏡表征 ······························ ············································································· 馬翩翩，劉觀福，喬 茵，徐人豪 （1 1 3）

釤鈷合金等溫時效過程中胞狀組織結(jié)構(gòu)的透射電鏡表征 ························································· ································································· 吳海辰，劉 壯，王新明，陳國新，盧煥明 （1 1 8）

導電環(huán)氧樹脂消除掃描電子顯微鏡圖像荷電問題的原理與實踐 ················································ ·············································································· 彭 宇，張之恒，安 婷，錢匡亮（1 2 5）

掃描電子顯微鏡在緩釋微球制劑表征中的應用進展 ················· 陳 超，樊海麗，蔡志威，張傳杰 （1 3 2）

pH調(diào)控水熱法合成BiVO4及其可見光催化降解甲基橙 ··········· 秦玉嬌，蔣琦銳，張智芝，王林霞 （1 3 9）

純鋅中變形孿晶界精細結(jié)構(gòu)的透射電子顯微鏡表征 ······························································· ····················································· 吳海辰，陳國新，于海濤，沈圣成，梁 芮，盧煥明 （2 4 7）

掃描電子顯微鏡和能譜分析高性能熱塑性板材 ····································································· ········································· 鄭 娜，徐 麗，沈素丹，賀 靜，房爾園，浦 群，介素云 （2 5 4）

掃描電子顯微鏡-能譜聯(lián)用在鑒別藥包材上的應用 ······························· 蔡志威，梁鍵謀，陳 超 （2 6 0）

新氫壓縮機活塞桿斷裂原因分析 ····· 姚懿容，蔣蓉蓉，段北晨，管建敏，熊發(fā)浩，李 明，盧煥明 （2 6 7）

掃描電子顯微鏡在鵪鶉蛋殼表征中的應用 ····················································· 鄭 希，戎念杭 （2 7 3）

掃描透射電子顯微鏡技術及其在中藥研究中的應用 ····················································· 王月霞 （2 8 0）

掃描電子顯微鏡運行和管理的實踐與探索 ····························· 何益超，盛國棟，陳朝貴，王林霞 （2 8 9）

*浙江省大型科研儀器開放共享平臺-大型科研儀器開放共享管理研究專欄

高校大型科研儀器開放共享運行機制探究 ········································· 亓文濤，陳 盼，高 然 （1 6 7）

高校和科研院所分析測試中心質(zhì)量管理體系重要性和建設舉措探究 ·········································· ································································· 張 麗，李子厚，陳 波，賈亞茹，戚淑燕 （1 7 3）

*研究報告

聚（異丙基甲基丙烯酰胺）@聚（N-異丙基丙烯酰胺）中空微凝膠合成過程的形態(tài)學表征 ··················· ············································································· 郭宏博，白 露，胡西學，孫 迪 （2 3 3）

脫氧核糖核酸變性和損傷的原子力顯微鏡液相觀察 ······························································· ··········································駱蕓爾，高 珊，伊 藝，陸 奕，鄭 寓，王艷偉，潘海鷗 （2 4 1）

*分析測試新方法

電感耦合等離子體質(zhì)譜法測定新型抗菌不銹鋼在生理鹽水和磷酸鹽緩沖液中的鎵溶出量 ··············· ························································································· 于英杰，李 輝，張重遠 （2 9 3）

無衍生化-氣相色譜法測定藥用膠塞提取液中硬脂酸和棕櫚酸 ·················································· ································································· 余秋玲，馬 艷，謝 威，楊 倩，龍 梅 （2 9 9）

離子色譜法快速測定氯化鉀中微量溴離子和硫酸根離子 ··································· 金 珍，閆春輝 （3 0 4）

*大型儀器功能開發(fā)

物理吸附系統(tǒng)的改造及其測試 ···················· 陳佩麗，王樹加，陳凱悅，陳曉麗，付 娟，蘇秋成 （3 9 2）